Research Paper:
Investigation of Effect of Cooling Rate on Mechanical Properties in Directed Energy Deposition
Yoko Hirono*,, Takanori Mori* , Hiroyuki Kawakami*, Masahiro Ueda*, and Daisuke Kono**
*DMG MORI Co., Ltd.
2-3-23 Shiomi, Koto-ku, Tokyo 135-0052, Japan
Corresponding author
**Graduate School of Engineering, Kyoto University
Kyoto, Japan
Directed energy deposition (DED) is one of the most promising additive manufacturing technologies, particularly for partial coating, repairing, and dissimilar metal depositing. However, determining the optimal deposition parameters to achieve desired shapes and mechanical properties is challenging because of the complex process of repeated melting and solidification driven by thermal energy. While some studies have focused on the cooling rate and its impact on mechanical properties, they have not evaluated the range within which the cooling rates vary. In this study, we investigated a range of cooling rates and their influence on hardness in DED under practical conditions using austenitic stainless steel SUS316L. The primary objective was to control the hardness of the deposited part by adjusting the cooling rate. Among the factors influencing hardness, grain size is particularly affected by cooling rates. Therefore, this study focused on grain size to evaluate the effects of DED technology. We proposed a method to calculate the cooling rate based on temperature distribution in the melt pool, captured by a camera coaxial with the laser beam. We varied the interpass dwell time, the resting interval between deposition layers, and investigated its effects on cooling rate and hardness. Additionally, the surface temperature of the workpiece during deposition was measured with a thermal camera. Results showed that while the dwell time did not significantly affect the calculated micro cooling rate, the deposition height had a notable impact. Conversely, the macroscopic temperature change was influenced by the dwell time. The cooling rate ranged from 3×103°C/s to 10×103°C/s, with hardness varying between 160 HV and 220 HV, and a linear correlation was observed between them.
- [1] M. K. Thompson, G. Moroni, T. Vaneker, G. Fadel, R. Campbel, I. Gibson, A. Bernard, J. Schulz, P. Graf, B. Ahuja, and F. Martina, “Design for Additive Manufacturing: Trends, Opportunities, Considerations, and Constraints,” Annals of the CIRP, Vol.65, No.2, pp. 737-760, 2016. https://doi.org/10.1016/j.cirp.2016.05.004
- [2] T. Furumoto, “Special Issue on Additive Manufacturing with Metals,” Int. J. Automation Technol., Vol.13, No.3, p. 329, 2019. https://doi.org/10.20965/ijat.2019.p0329
- [3] M. Schmidt, M. Merklein, D. Bourell, D. Dimitrov, T. Hausotte, K. Wegener, L. Overmeyer, F. Vollertsen, and G. N. Levy, “Laser based additive manufacturing in industry and academia,” Annals of the CIRP, Vol.66, No.2, pp. 561-583, 2017. https://doi.org/10.1016/j.cirp.2017.05.011
- [4] R. Koike, I. Unotoro, Y. Kakinuma, and Y. Oda, “Graded Inconel 625 – SUS316L Joint Fabricated Using Directed Energy Deposition,” Int. J. Automation Technol., Vol.13, No.3, pp. 338-345, 2019. https://doi.org/10.20965/ijat.2019.p0338
- [5] J. Tuominen, M. Kaubisch, S. Thieme, J. Nakki, S. Nowotny, and P. Vuoristo, “Laser strip cladding for large area metal deposition,” Additive Manufacturing, Vol.27, pp. 208-216, 2019. https://doi.org/10.1016/j.addma.2019.01.008
- [6] S. Cecchel, D. Ferrario, C. Mondini, M. Montani, and B. Previtali, “Application of Laser Metal Deposition for a New Model of Assembled Camshaft,” J. Mater. Eng. Perform., Vol.28, pp. 7756-7767, 2019. https://doi.org/10.1007/s11665-019-04504-2
- [7] G. Y. Baek, G. Y. Shin, K. Y. Lee, and S. Shim, “Mechanical Properties of Tool Steels with High Wear Resistance via Directed Energy Deposition,” Metals, Vol.9, No.3, Article No.9030282, 2019. https://doi.org/10.3390/met9030282
- [8] J. S. Zuback and T. DebRoy, “The Hardness of Additively Manufactured Alloys,” Materials, Vol.11, Article No.11112070, 2018. https://doi.org/10.3390/ma11112070
- [9] L. Costa, R. Vilar, T. Reti, and A. M. Deus, “Rapid tooling by laser powder deposition: Process simulation using finite element analysis,” Acta Materialia, Vol.53, No.14, pp. 3987-3999, 2005. https://doi.org/10.1016/j.actamat.2005.05.003
- [10] Y. Li, Y. Wang, J. Niu, S. Liu, Y. Lin, N. Liu, J. Ma, Z. Zhang, and J. Wang, “Microstructure and mechanical properties of M2 high speed steel produced by electron beam melting,” Materials Science and Engineering: A, Vol.862, Article No.144327, 2023. https://doi.org/10.1016/j.msea.2022.144327
- [11] M. H. Farshidianfar, F. Khodabakhshi, A. Khajepour, and A. P. Gerlich, “Closed-loop control of microstructure and mechanical properties in additive manufacturing by directed energy deposition,” Materials Science and Engineering: A, Vol.803, Article No.140483, 2021. https://doi.org/10.1016/j.msea.2020.140483
- [12] M. H. Farshidianfar, A. Khajepour, and A. Gerlich, “Real-time control of microstructure in laser additive manufacturing,” The Int. J. of Advanced Manufacturing Technology, Vol.82, pp. 1173-1186, 2016. https://doi.org/10.1007/s00170-015-7423-5
- [13] A. Emamian, M. Alimardani, and A. Khajepour, “Effect of cooling rate and laser process parameters on additive manufactured Fe–Ti–C metal matrix composites microstructure and carbide morphology,” J. of Manufacturing Processes, Vol.16, pp. 511-517, 2014. https://doi.org/10.1016/j.jmapro.2014.07.002
- [14] Y. Huang, M. Ansari, H. Asgari, M. H. Farshidianfar, D. Sarker, M. B. Khamesee, and E. Toyserkani, “Rapid prediction of real-time thermal characteristics, solidification parameters and microstructure in laser directed energy deposition (powder-fed additive manufacturing),” J. of Materials Processing Technology, Vol.274, Article No.116286, 2019. https://doi.org/10.1016/j.jmatprotec.2019.116286
- [15] H. Kim, K.-K. Lee, D.-G. Ahn, and H. Lee, “Effects of Deposition Strategy and Preheating Temperature on Thermal-Mechanical Characteristics of Inconel 718 Super-Alloy Deposited on AISI 1045 Substrate Using a DED Process,” Materials, Vol.14, Article No.14071794, 2021. https://doi.org/10.3390/ma14071794
- [16] K. Ren, Y. Chew, J. Y. H. Fuh, Y. F. Zhang, and G. J. Bi, “Thermo-mechanical analyses for optimized path planning in laser aided additive manufacturing processes,” Materials & Design, Vol.162, pp. 80-93, 2019. https://doi.org/10.1016/j.matdes.2018.11.014
- [17] M. P. Sefidi, R. Israr, J. Buhl, and M. Bambach, “Rule-Based Path Identification for Direct Energy Deposition,” Procedia Manufacturing, Vol.47, pp. 1134-1140, 2020. https://doi.org/10.1016/j.promfg.2020.04.133
- [18] C. Guévenoux, S. Hallais, A. Charles, E. Charkaluk, and A. Constantinescu, “Influence of interlayer dwell time on the microstructure of Inconel 718 Laser Cladded components,” Optics & Laser Technology, Vol.128, Article No.106218, 2020. https://doi.org/10.1016/j.optlastec.2020.106218
- [19] C. Kledwig, H. Perfahl, M. Reisacher, F. Brückner, J. Bliedtner, and C. Leyens, “Analysis of Melt Pool Characteristics and Process Parameters Using a Coaxial Monitoring System during Directed Energy Deposition in Additive Manufacturing,” Materials, Vol.12, Article No.12020308, 2019. https://doi.org/10.3390/ma12020308
- [20] J. Caniou, “Passive Infrared Detection: Theory and Applications,” Dordrecht: Kluwer Academic Publishers, p. 166, 1999. https://doi.org/10.1007/978-1-4757-6140-5
- [21] Japanese Industrial Standard, “Steels – Micrographic determination of the apparent grain size,” JIS G 0551:2020, 2020.
- [22] N. Hirota, F. Yin, T. Inoue, and T. Azuma, “Recrystallization and Grain Growth Behavior in Severe Cold-rolling Deformed SUS316L Steel under Anisothermal Annealing Condition,” ISIJ Int., Vol.48, No.4, pp. 475-482, 2008. https://doi.org/10.2355/isijinternational.48.475
- [23] X. Zhao, Y. Liu, Y. Wang, P. Feng, and H. Tang, “Recrystallization and Grain Growth of 316L Stainless Steel Wires,” Metallurgical and Materials Trans. A, Vol.45, pp. 3446-3453, 2014. https://doi.org/10.1007/s11661-014-2305-2
- [24] R. Vilar, “Laser cladding,” J. of Laser Applications, Vol.11, pp. 64-79, 1999. https://doi.org/10.2351/1.521888
This article is published under a Creative Commons Attribution-NoDerivatives 4.0 Internationa License.